1-(Bromomethyl)-4-(1,1-dimethylethyl)benzene → HCID 68987285, compound

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Also, N-cyclopropyl-N-[1-(4-tert-butylbenzyl)piperidin-4-yl]-benzenesulfonamide was prepared from N-cyclopropyl-N-piperidin-4-yl-benzenesulfonamide and 1-bromomethyl-4-tert-butylbenzene. LC: 100%, MS: m/z=427.2, 428.3 (M+H+). 1H NMR (400 MHz, CDCl3): δ 7.85 (2H, m), 7.56 (1H, m), 7.50 (2H, m), 7.32 (2H, d, J=8.4 Hz), 7.19 (2H, d, J=8.4 Hz), 3.85 (1H, m), 3.44 (2H, s), 2.89 (1H, s), 2.87 (1H, s), 1.97 (5H, m), 1.59 (4H, s), 1.49 (1H, s), 1.47 (1H, s), 1.32 (9H, s), 0.97 (2H, m), 0.75 (2H, m).

Provenance & Evidence