Phenylboronic Acid → HCID 59575284, compound

HRID 1468600Notes

Reaction equation

HRID 1468600 reaction equation
FC(F)(F)S(O[C:7]1[N:8]=[CH:9][C:10]2[C:15]([CH:16]=1)=[C:14]1[CH:17]=[CH:18][CH:19]=[CH:20][C:13]1=[C:12]1[CH:21]=[CH:22][CH:23]=[CH:24][C:11]=21)(=O)=O.[C:27]1(B(O)O)[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1>>[C:27]1([C:7]2[N:8]=[CH:9][C:10]3[C:15]([CH:16]=2)=[C:14]2[CH:17]=[CH:18][CH:19]=[CH:20][C:13]2=[C:12]2[CH:21]=[CH:22][CH:23]=[CH:24][C:11]=32)[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1

Participants

3

Reactant 2

HCID 66827Phenylboronic AcidHCID 59575351HCID 59575351, compound

Product 1

HCID 59575284HCID 59575284, compound

Procedure

Dibenzo[f,h]isoquinolin-3-yl trifluoromethanesulfonate compound as synthesized in above Step 4 of Compound 1 synthesis reacts with phenylboronic acid under Suzuki reaction condition as described in Step 7 of Compound 1 synthesis to give the ligand 3-phenyldibenzo[f,h]isoquinoline.

Sources & evidence

ORD record
ord-7e8380711cba44d3949aa8d0969d2693
Source dataset
uspto-grants-2015_04
Patent number
US09005771B2

Reaction notes

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