HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropanemethanamine → HCID 71468903, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropanemethanamine | HCID 75646 | — |
| Reactant | 1-Propanamine, N-[2-[3-fluoro-5-(methylsulfonyl)phenoxy]ethyl]- | HCID 70980485 | — |
| Reactant | HCID 86717739 | HCID 86717739 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 71468903 | HCID 71468903 | — |
Reaction Steps
Preparation according to Example 1 but performed in one portion: 1-(2-bromoethoxy)-3-fluoro-5-methylsulfonyl-benzene (0.05 g, 0.16 mmol) and aminomethylcyclopropane (0.11 ml, 1.3 mmol) in ethanol (5 ml). MS m/z (relative intensity, 70 eV) 287 (M+, 2), 246 (6), 138 (2), 84 (bp), 56 (14).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09006227B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-8bfe252a05ef4cdb87382d89901bd261 |
| Source note | uspto-grants-2015_04 |