HRID1468835

反应详情

EQUATION

反应方程式

HRID 1468835 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

The product of step A (170 mg, 0.62 mmol) and 5% Pd/C (20 mg) were dissolved in EtOH (5 mL). The mixture was stirred under 1 atm of H2 for 1 hour. The mixture was filtered and the filtrate concentrated in vacuo, yielding the title compound.

WORKUP

后处理

  1. filtrationThe mixture was filtered
  2. concentrationthe filtrate concentrated in vacuo