HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus pentachloride → HCID 86692242, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | HCID 136336821 | HCID 136336821 | — |
| Solvent | Phosphorus oxychloride | HCID 24813 | — |
| Product | HCID 86692242 | HCID 86692242 | 186.7% |
Reaction Steps
The title compound was prepared following the procedure described in Intermediate-7, step-2 using 8-nitro-2-(trifluoromethyl)quinazolin-4(3H)-one (500 mg, 1.93 mmol) and PCl5 (477 mg, 2.32 mmol) in POCl3 (2.5 mL) to afford 1.0 g of the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09006257B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-d57db63180a8429a9f2869aa36143f81 |
| Source note | uspto-grants-2015_04 |