2-Bromoethyl methyl ether → HCID 178465757, compound

HRID 1469965Notes

Reaction equation

HRID 1469965 reaction equation
[CH2:1]([O:3][C:4]12[CH2:11][O:10][CH2:9][CH:8]1[S:7][C:6]([NH:12][C:13]([C:15]13[CH2:24][CH:19]4[CH2:20][CH:21]([CH2:23][CH:17]([CH2:18]4)[CH2:16]1)[CH2:22]3)=[O:14])=[N:5]2)[CH3:2].[CH3:25][O:26][CH2:27][CH2:28]Br>>[CH2:1]([O:3][C:4]12[CH2:11][O:10][CH2:9][CH:8]1[S:7]/[C:6](=[N:12]\[C:13]([C:15]13[CH2:24][CH:19]4[CH2:20][CH:21]([CH2:23][CH:17]([CH2:18]4)[CH2:16]1)[CH2:22]3)=[O:14])/[N:5]2[CH2:28][CH2:27][O:26][CH3:25])[CH3:2]

Participants

3

Reactant 2

HCID 809722-Bromoethyl methyl etherHCID 67095536Adamantane-1-carboxylic acid (3a-ethoxy-3a,4,6,6a-tetrahydro-furo[3,4-d]thiazol-2-yl)-amide

Product 1

HCID 178465757HCID 178465757, compound

Procedure

The product of Example 72C and 2-bromoethyl methyl ether were processed according to the method of Example 1B to afford the title compound. MS (ESI+) m/z 409 (M+H)+.

Sources & evidence

ORD record
ord-9dd7eaecab7f42e69e80c2542beb8df7
Source dataset
uspto-grants-2015_04
Patent number
US09006275B2

Reaction notes

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