HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-4,5-dimethyl-1,3-thiazole → HCID 131728627, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-4,5-dimethyl-1,3-thiazole | HCID 73238 | — |
| Reactant | tert-Butyl bromoacetate | HCID 79177 | — |
| Product | HCID 131728627 | HCID 131728627 | — |
Reaction Steps
Bromoacetic acid tert-butyl ester (1.4 mL, 9.4 mmol) and 4,5-dimethyl-2-aminothiazole (1.0 g, 7.8 mmol) were heated at 85° C. for 14 hours. The mixture was cooled to ambient temperature and the resulting solid was triturated with ethyl acetate to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09006275B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-96c071917e3a465c8f8a5a08a8f6d4ce |
| Source note | uspto-grants-2015_04 |