HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiourea → 4-Cyclopropyl-1,3-thiazol-2-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiourea | HCID 2723790 | — |
| Reactant | 2-Bromo-1-cyclopropylethan-1-one | HCID 10920841 | — |
| Product | 4-Cyclopropyl-1,3-thiazol-2-amine | HCID 674456 | — |
Reaction Steps
A mixture of 2-bromo-1-cyclopropyl-ethanone (0.50 g, 3.0 mmol, Waterstone Technology) and thiourea (0.23 g, 3.1 mmol) were processed as in Example 71A to afford the title compound. MS (DCI/NH3) m/z 141 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09006275B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-9323089e99744939ac669f41f9acc856 |
| Source note | uspto-grants-2015_04 |