関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 2-Chlorocyclopentanone | HCID 12751 | — |
| 反応物 | Thiourea | HCID 2723790 | — |
| 生成物 | 5,6-Dihydro-4H-cyclopenta[d]thiazol-2-amine hydrochloride | HCID 16253246 | — |
反応手順
A mixture of 2-chlorocyclopentanone (5.00 g, 39.5 mmol) and thiourea (3.00 g, 39.5 mmol) was heated at 80° C. for 3-4 minutes. After cooling to room temperature, the mixture was triturated with ethanol and the solid was collected by filtration to afford the title compound. MS (ESI) m/z 141 (M+H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US09006275B2 |
|---|
| 出典データセット | uspto-grants-2015_04 |
|---|
| ORD ID | ord-dde4693a6dad4f318db8fad5048e711a |
|---|
| 出典メモ | uspto-grants-2015_04 |
|---|
