Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1470394Generated: November 1, 2026

4,5,6,7-Tetrahydro-benzo[b]thiophene-2-carbonyl chloride → HCID 66779332, compound

https://huagongshe.com/reaction/1470394

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4,5,6,7-Tetrahydro-benzo[b]thiophene-2-carbonyl chlorideHCID 6485362—
ReactantHCID 86694440HCID 86694440—
ProductHCID 66779332HCID 66779332—

Reaction Steps

The compound was synthesized according to the procedure M using 2-methyl-3-{2-[4-(pyrrolidin-1-ylcarbonyl)phenyl]furo[3,2-b]pyridin-7-yl}aniline (40.00 mg, 0.10 mmol) and 4,5,6,7-tetrahydro-1-benzothiophene-2-carbonyl chloride (22.22 mg, 0.11 mmol). The title compound was obtained as a white solid (8.00 mg, 14%). HPLC (method F): 82%, RT=4.365. MS: m/z=562 [M+H]+, RT=4.33 min.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09006440B2
Source datasetuspto-grants-2015_04
ORD IDord-2da24e84efa64faba7bf7d1fd6e514c3
Source noteuspto-grants-2015_04