HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,5,6,7-Tetrahydro-benzo[b]thiophene-2-carbonyl chloride → HCID 66779332, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,5,6,7-Tetrahydro-benzo[b]thiophene-2-carbonyl chloride | HCID 6485362 | — |
| Reactant | HCID 86694440 | HCID 86694440 | — |
| Product | HCID 66779332 | HCID 66779332 | — |
Reaction Steps
The compound was synthesized according to the procedure M using 2-methyl-3-{2-[4-(pyrrolidin-1-ylcarbonyl)phenyl]furo[3,2-b]pyridin-7-yl}aniline (40.00 mg, 0.10 mmol) and 4,5,6,7-tetrahydro-1-benzothiophene-2-carbonyl chloride (22.22 mg, 0.11 mmol). The title compound was obtained as a white solid (8.00 mg, 14%). HPLC (method F): 82%, RT=4.365. MS: m/z=562 [M+H]+, RT=4.33 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09006440B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-2da24e84efa64faba7bf7d1fd6e514c3 |
| Source note | uspto-grants-2015_04 |