Lithium Hydroxide → HCID 57692808, compound

HRID 1470686Notes

Reaction equation

HRID 1470686 reaction equation
[Li+].[OH-].[Cl:3][C@H:4]1[C@H:8]([CH2:9][CH2:10][S:11][C:12]2[S:13][CH:14]=[C:15]([C:17]([O:19]CC)=[O:18])[N:16]=2)[C@@H:7]([CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29])[C@H:6]([OH:30])[CH2:5]1>>[Cl:3][C@H:4]1[C@H:8]([CH2:9][CH2:10][S:11][C:12]2[S:13][CH:14]=[C:15]([C:17]([OH:19])=[O:18])[N:16]=2)[C@@H:7]([CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29])[C@H:6]([OH:30])[CH2:5]1

Participants

3

Reactant 2

HCID 3939Lithium HydroxideHCID 68926119HCID 68926119, compound

Product 1

HCID 57692808HCID 57692808, compoundYield 106.7%

Procedure

The previously described LiOH procedure (U.S. Pat. No. 7,091,231) was used, starting with 13 mg 6-7 and providing 6-8 (13 mg, 100%).

Sources & evidence

ORD record
ord-623aca90a68d40ad829292c449f6d7ce
Source dataset
uspto-grants-2015_04
Patent number
US09006464B2

Reaction notes

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