Hydrochloric Acid → HCID 67125457, compound

Participants

Reaction Conditions

Reaction Steps

11.3 mL (14.1 mmol) 1.25 N HCl in methanol are added to 900 mg (2.12 mmol) (S)-(1-{4-[1-(4-ethoxy-phenyl)-piperidin-4-yl]-phenyl}-ethyl)-carbamic acid tert-butyl ester (XII.1) in 25 mL dichloromethane. The mixture is stirred for 14 h at rt and for 1 h at 50° C. After that time, the solvent is removed in vacuo to yield the desired product.

Provenance & Evidence