HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 67125425, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | HCID 67125383 | HCID 67125383 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 67125425 | HCID 67125425 | — |
Reaction Steps
To 9.60 g (37.7 mmol) (S)—N-[1-(4-pyridin-4-yl-phenyl)-ethyl]-propionamide (IV.6) in 120 mL acetone are added 4.91 mL (41.5 mmol) benzyl bromide. The mixture is refluxed for 12 h. After that time, the precipitate is filtered off, washed with acetone and dried at 50° C. to yield the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09006450B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-00ddd8b6d4294c2383da69ed4fcd403c |
| Source note | uspto-grants-2015_04 |