HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1470764Generated: October 30, 2026
HCID 67125450, compound → HCID 67125411, compound
https://huagongshe.com/reaction/1470764
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 67125450 | HCID 67125450 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 67125411 | HCID 67125411 | — |
Reaction Steps
A mixture of 92 mg (S)-2-{4-[4-(1-acetylamino-ethyl)-phenyl]-piperidin-1-yl}-pyrimidine-5-carboxylic acid (2-amino-phenyl)-amide in 2 mL HOAc is refluxed for 12 h at 110° C. After concentration in vacuo water is added and the precipitate is collected by filtration to yield the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09006450B2 |
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| Source dataset | uspto-grants-2015_04 |
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| ORD ID | ord-d8e8ef4dd5534cfa92a796a010ec71c5 |
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| Source note | uspto-grants-2015_04 |
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