2-Ethylhexanoyl chloride → HCID 86692648, compound

Participants

Reaction Steps

2.31 mmol of AlCl3 was added to 20 ml DCM with 2.31 mmol 2-ethylhexanoyl chloride at about 0° C. Compound 7 from the previous step was added to the mixture. The mixture was reacted at about 0° C. for about 4 hours. After reacting, the reactant was poured into ice water. The organic phase was extracted by ether 3 times. Compound 8 was purified by silica gel. The yield was about 70%.

Provenance & Evidence