HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 68725716, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | HCID 68724806 | HCID 68724806 | — |
| Product | HCID 68725716 | HCID 68725716 | 69% |
Reaction Steps
Prepared in 69% yield from 3-hydroxy-1-(7-methylspiro[4.5]deca-6,8-dien-6-yl)butan-1-one (1.88 g, 8.0 mmol), acetic anhydride (1.6 ml) and sodium acetate (0.72 g) as described in Example 10. Boiling point: 120° C. (0.09 mbar).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09012391B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-cc9c7d950fc441b2a6b301fd442dab42 |
| Source note | uspto-grants-2015_04 |