HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1471809Generated: October 30, 2026
Diethyl (ethoxymethylene)malonate → HCID 67281873, compound
https://huagongshe.com/reaction/1471809
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diethyl (ethoxymethylene)malonate | HCID 6871 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 67282538 | HCID 67282538 | — |
| Product | HCID 67281873 | HCID 67281873 | — |
Reaction Steps
Equimolar ratios of ethyl 3-methyl-1H-pyrrole-2-carboxylate hydrochloride, diisopropylethylamine and diethyl ethoxymethylenemalonate were mixed in a sealed tube and heated at 100° C. for 15 hours. After cooling to room temperature, column chromatography afforded the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09012470B2 |
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| Source dataset | uspto-grants-2015_04 |
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| ORD ID | ord-d46d0281a52a4db4a7aa719cbc4d2d53 |
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| Source note | uspto-grants-2015_04 |
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