HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 16875682, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methyl 4-(4-methylpiperazin-1-yl)-3-nitrobenzoate | HCID 2904229 | — |
| Product | HCID 16875682 | HCID 16875682 | — |
Reaction Steps
A solution of 4-(4-methyl-piperazin-1-yl)-3-nitro-benzoic acid methyl ester (1.8 g, 6.4 mmol) in 35 mL of 5N HCl was stirred at 55° C. for 16 h. The reaction mixture was then evaporated to dryness affording the title compound (quantitative) that was used for the next step without any further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09012487B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-b261e6031b1d4ce8b069f04ecf68ee10 |
| Source note | uspto-grants-2015_04 |