HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Dihydroxyboranyl)-3-fluorobenzoic acid → HCID 66980029, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Dihydroxyboranyl)-3-fluorobenzoic acid | HCID 23134177 | — |
| Reactant | 2,3-Dichloro-6-methoxyquinoline | HCID 39733293 | — |
| Product | HCID 66980029 | HCID 66980029 | — |
Reaction Steps
Scheme 3: starting from 2,3-dichloro-6-methoxyquinoline (Intermediate 4) and 4-borono-3-fluorobenzoic acid. An aqueous/EtOAc workup was performed followed by purification by silica gel column (PE/EtOAc=1/1) to give the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09012646B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-3554f2711fac4950a9bd54dbb0221436 |
| Source note | uspto-grants-2015_04 |