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HRID1472696

反应详情

EQUATION

反应方程式

HRID 1472696 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[Na+].[Na+]
HCID10340

Carbonic acid sodium salt (1:2)

CNa2O3

结构：COC(=O)c1ccc(B(O)O)cc1
HCID2734369

[4-(Methoxycarbonyl)phenyl]boronic acid

C8H9BO4

结构：COc1ccc2cc(Br)cnc2c1
HCID18788548

3-Bromo-7-methoxyquinoline

C10H8BrNO

PRODUCTS

生成物

1
结构：COC(=O)c1ccc(-c2cnc3cc(OC)ccc3c2)cc1
HCID67974241

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：COCCOC.O
溶剂HCID18180031

未命名化合物

PROCEDURE

实验过程

Followed Step 1 of Compound IV-1, starting from 4-(methoxycarbonyl)phenylboronic acid and Intermediate 13, and where the base used was Na2CO3, the solvent DME/H2O (8: 2), and the reaction was run at 100° C. for 2 h.