HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59238245, compound → (3-bromo-2,5-dimethylphenyl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59238245 | HCID 59238245 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | (3-bromo-2,5-dimethylphenyl)methanol | HCID 10656303 | — |
Reaction Steps
To a solution of 3-bromo-2,5-dimethylbenzoic acid (3.5 g, 15 mmol) in anhydrous THF was added borane THF complex (1.0 M, 25 mL, 25 mmol) at 0, then the reaction was warmed to ambient temperature overnight. The reaction was quenched with MeOH and concentrated to afford (3-bromo-2,5-dimethylphenyl)methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09018211B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-7493043f55034c139b232a4efd223ef5 |
| Source note | uspto-grants-2015_04 |