HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorobutylbutyrate → 1-(Butyryloxy)butyl-5-amino-4-oxopentanoate Hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorobutylbutyrate | HCID 15094345 | — |
| Reactant | 5-((tert-Butoxycarbonyl)amino)-4-oxopentanoic acid | HCID 17989820 | — |
| Product | 1-(Butyryloxy)butyl-5-amino-4-oxopentanoate Hydrochloride | HCID 86709205 | — |
Reaction Steps
The compound was prepared as described in Procedures A and B above from 2-chlorobutylbutyrate and 5-(tert-butoxycarbonylamino)-4-oxopentanoic acid. 1H-NMR (300 MHz, CD3OD) ppm δ 0.95+0.96 (two t, J=6.6 Hz, 6H, two Me), 1.65 (m, 6H, CH3CH2CH2CO2+CH3CH2CH2CH), 2.27 (t, J=10.8 Hz, 2H, CH2CH2CH2CO2), 2.70 (“t”, 2H, COCH2CH2CO2), 2.87 (“t”, 2H, COCH2CH2CO2), 4.02 (s, 2H, CH2NH2), 6.72 (t, J=8.4 Hz, 1H, OCHO).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09018257B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-96b4af036c6d4a1d95eca331bb254bf4 |
| Source note | uspto-grants-2015_04 |