HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfide → HCID 90231912, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfide | HCID 1068 | — |
| Reactant | HCID 70982021 | HCID 70982021 | — |
| Product | HCID 90231912 | HCID 90231912 | 67.4% |
Reaction Steps
3-Benzyl-6-chloro-3-methyl-1,3-dihydro-indol-2-one (641 mg) was reduced with BH3.Me2S following a similar method to that described in Preparation 54 to give title compound (410 mg) as a colourless gum. MS: [M+H]+=258.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09018214B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-47e19044a9534be6b8d1ca76ad3f3ad6 |
| Source note | uspto-grants-2015_04 |