HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70980247, compound → HCID 70980544, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70980247 | HCID 70980247 | — |
| Catalyst | Iron | HCID 23925 | — |
| Product | HCID 70980544 | HCID 70980544 | 59.1% |
Reaction Steps
Following similar methods to those described in Preparation 326 starting from 2-(4-bromo-2-nitro-phenyl)-2-phenyl-propionic acid methyl ester (1.3 g, 4.9 mmol) and iron powder (890 mg, 15 mmol) gave the title compound (875 mg) as a yellow solid. MS: [M+H]+=302.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09018214B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-7caa7c29231e4844bf46e8524517a9bf |
| Source note | uspto-grants-2015_04 |