Trifluoroacetic acid → HCID 86667527, compound

Participants

Reaction Steps

22.0 mg (0.040 mmol) of tert-butyl 1-(4-chloro-3-{[(2S,3R)-2-(4-chlorophenyl)-4,4,4-trifluoro-3-methylbutanoyl]amino}-2-fluorobenzyl)cyclopropanecarboxylate were dissolved in 0.19 ml of dichloromethane, and 0.5 ml of TFA was added at RT. After 1 h at RT, the reaction mixture was concentrated under reduced pressure and the residue was dried under high vacuum overnight. This gave 17.8 mg (82.2% of theory) of the target compound.

Provenance & Evidence