Potassium Carbonate → HCID 11311797, compound

HRID 1475729Notes

Reaction equation

HRID 1475729 reaction equation
[CH2:1]([O:3][C:4](=[O:23])[C:5]1[CH:10]=[CH:9][C:8]([O:11][CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[C:7]([O:19]C(=O)C)[CH:6]=1)[CH3:2].C(=O)([O-])[O-].[K+].[K+]>CO>[CH2:1]([O:3][C:4](=[O:23])[C:5]1[CH:10]=[CH:9][C:8]([O:11][CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[C:7]([OH:19])[CH:6]=1)[CH3:2]

Participants

4

Reactant 2

HCID 11430Potassium CarbonateHCID 67170201HCID 67170201, compound

Product 1

HCID 11311797HCID 11311797, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The compound of step 2 (10 g, 31.8 mmol) was dissolved in methanol, potassium carbonate (88 mg, 0.636 mmol) was added and the mixture was stirred for 2 h under reflux. The solution was evaporated to dryness and the residue used without further purification.

Workup

  1. temperatureunder reflux
  2. customThe solution was evaporated to dryness
  3. customthe residue used without further purification

Sources & evidence

ORD record
ord-d90752650c4f472285caa383b64c714a
Source dataset
uspto-grants-2015_04
Patent number
US09018383B2

Reaction notes

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