HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 53240895, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 2-Methanesulfonylbenzene-1-sulfonyl chloride | HCID 2735178 | — |
| Reactant | (Acetyloxy)-carbamic acid tert-butyl ester | HCID 10058028 | — |
| Product | HCID 53240895 | HCID 53240895 | — |
Reaction Steps
tert-Butyl (acetyloxy){[2-(methylsulfonyl)phenyl]sulfonyl}carbamate (42) is prepared from 2-methylsulfonylbenzenesulfonyl chloride, sodium hydride and [(tert-butoxy)carbonyl]amino acetate according to Scheme 2. (0.5 g, 16%), 1H NMR (400 MHz, DMSO-d6) δ ppm 8.26-8.34 (1H, m), 8.17-8.25 (1H, m), 8.03-8.11 (2H, m), 3.46 (3H, s), 2.32 (3H, s), 1.28 (9H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09018411B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-fc792dcd52e44b03ac1673f1773b6cfd |
| Source note | uspto-grants-2015_04 |