HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propionyl chloride → HCID 17825483, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propionyl chloride | HCID 62324 | — |
| Reactant | tert-butyl N-hydroxycarbamate | HCID 97534 | — |
| Product | HCID 17825483 | HCID 17825483 | — |
Reaction Steps
[(tert-Butoxy)carbonyl]amino propanoate is prepared from propionyl chloride and N-tert-butoxycarbonyl hydroxylamine according to Scheme 1 described by Carpino et al. J. Am. Chem. Soc. 1959, 955-957. (3.4 g, 48%), 1H NMR (250 MHz, DMSO-d6) δ ppm 10.57 (1H, br. s.), 2.40 (2H, q, 7.5 Hz), 1.40 (9H, s), 1.07 (3H, t, 7.4 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09018411B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-512ed0cf4d124a35a142cac98fcadd0c |
| Source note | uspto-grants-2015_04 |