HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetyl chloride → HCID 86654173, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetyl chloride | HCID 7679 | — |
| Reactant | tert-butyl N-hydroxycarbamate | HCID 97534 | — |
| Product | HCID 86654173 | HCID 86654173 | — |
Reaction Steps
[(tert-Butoxy)carbonyl]amino 2-phenylacetate is prepared from phenylacetyl chloride and N-tert-butoxycarbonyl hydroxylamine according to Scheme 1 using literature conditions. (8.8 g, 100%), 1H NMR (500 MHz, DMSO-d6) δ ppm 10.66 (1H, br. s.), 7.24-7.38 (5H, m), 3.80 (2H, s), 1.38 (9H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09018411B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-4721a10814fb4e22b5c936e500f14a2d |
| Source note | uspto-grants-2015_04 |