Dimethylcarbamoyl Chloride → HCID 21098732, compound

HRID 1476000Notes

Reaction equation

HRID 1476000 reaction equation
[OH:1][NH:2][C:3](=[O:9])[O:4][C:5]([CH3:8])([CH3:7])[CH3:6].[CH3:10][N:11]([CH3:15])[C:12](Cl)=[O:13]>>[CH3:10][N:11]([CH3:15])[C:12](=[O:13])[O:1][NH:2][C:3]([O:4][C:5]([CH3:8])([CH3:7])[CH3:6])=[O:9]

Participants

3

Reactant 2

HCID 6598Dimethylcarbamoyl ChlorideHCID 97534tert-butyl N-hydroxycarbamate

Product 1

HCID 21098732HCID 21098732, compound

Procedure

[(tert-Butoxy)carbonyl]amino N,N-dimethylcarbamate is prepared from tert-butyl N-hydroxycarbamate and dimethyl carbamoyl chloride according to Scheme 1. (2.4 g, 78%), 1H NMR (500 MHz, CHLOROFORM-d) δ ppm 7.82 (1H, br. s.), 3.02 (3H, s), 2.98 (3H, s), 1.49 (9H, s)

Sources & evidence

ORD record
ord-8b8fe6f556e847ef888e42d3f459f35a
Source dataset
uspto-grants-2015_04
Patent number
US09018411B2

Reaction notes

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