HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylcarbamoyl chloride → HCID 86654178, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylcarbamoyl chloride | HCID 6916 | — |
| Reactant | tert-butyl N-hydroxycarbamate | HCID 97534 | — |
| Product | HCID 86654178 | HCID 86654178 | — |
Reaction Steps
[(tert-Butoxy)carbonyl]amino N,N-diethylcarbamate is prepared from tert-butyl N-hydroxycarbamate and diethyl carbamoyl chloride according to Scheme 1. (0.67 g, 39%), 1H NMR (500 MHz, CHLOROFORM-d) δ ppm 7.84 (1H, br. s.), 3.33 (4H, q, 7.1 Hz), 1.48 (9H, s), 1.11-1.28 (6H, m).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09018411B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-25009dddb78b43dbb1b3d3a0e1f7d94a |
| Source note | uspto-grants-2015_04 |