tert-butyl N-hydroxycarbamate → HCID 86654179, compound

HRID 1476003Notes

Reaction equation

HRID 1476003 reaction equation
[OH:1][NH:2][C:3](=[O:9])[O:4][C:5]([CH3:8])([CH3:7])[CH3:6].[CH3:10][O:11][N:12]([CH3:16])[C:13](Cl)=[O:14]>>[CH3:10][O:11][N:12]([CH3:16])[C:13](=[O:14])[O:1][NH:2][C:3]([O:4][C:5]([CH3:8])([CH3:7])[CH3:6])=[O:9]

Participants

3

Reactant 2

HCID 97534tert-butyl N-hydroxycarbamateHCID 2734926N-methoxy-N-methylcarbamoyl chloride

Product 1

HCID 86654179HCID 86654179, compound

Procedure

[(tert-Butoxy)carbonyl]amino N-methoxy-N-methylcarbamate is prepared from tert-butyl N-hydroxycarbamate and N-Methoxy-N-methylcarbamoyl chloride according to Scheme 1. (2.48 g, 100%), 1H NMR (500 MHz, CHLOROFORM-d) δ ppm 7.83 (1H, s), 3.76 (3H, s), 3.23 (3H, s), 1.48 (9H, s).

Sources & evidence

ORD record
ord-a52cd145f95748979ef3b6ec5368c23c
Source dataset
uspto-grants-2015_04
Patent number
US09018411B2

Reaction notes

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