HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-butyl N-hydroxycarbamate → HCID 86654179, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-butyl N-hydroxycarbamate | HCID 97534 | — |
| Reactant | N-methoxy-N-methylcarbamoyl chloride | HCID 2734926 | — |
| Product | HCID 86654179 | HCID 86654179 | — |
Reaction Steps
[(tert-Butoxy)carbonyl]amino N-methoxy-N-methylcarbamate is prepared from tert-butyl N-hydroxycarbamate and N-Methoxy-N-methylcarbamoyl chloride according to Scheme 1. (2.48 g, 100%), 1H NMR (500 MHz, CHLOROFORM-d) δ ppm 7.83 (1H, s), 3.76 (3H, s), 3.23 (3H, s), 1.48 (9H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09018411B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-a52cd145f95748979ef3b6ec5368c23c |
| Source note | uspto-grants-2015_04 |