Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydroxylamine | HCID 787 | — |
| Reactant | 66502-25-8 | HCID 18980923 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 43248107 | HCID 43248107 | — |
Reaction Steps
A mixture of propoxyacetonitrile (3.03 g) and hydroxylamine (2.01 g, 50 wt % in water) is stirred for 2 h at 100° C. At RT DCM is added, the organic phase is separated, dried over sodium sulfate and concentrated under reduced pressure to give the title compound as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09018175B2 |
|---|
| Source dataset | uspto-grants-2015_04 |
|---|
| ORD ID | ord-1489afd5ce5c4c1e95fdd821af9fbff7 |
|---|
| Source note | uspto-grants-2015_04 |
|---|
