Hydroxylamine → HCID 24697443, compound
Reaction equation
[CH3:1][O:2][CH2:3][CH2:4][CH2:5][C:6]#[N:7].[NH2:8][OH:9]>>[OH:9]/[N:8]=[C:6](\[NH2:7])/[CH2:5][CH2:4][CH2:3][O:2][CH3:1]Participants
3
Procedure
In analogy to the procedure described for example D28 4-methoxybutanenitrile (3.1 g) and hydroxylamine (2.07 g, 50 wt % in water) yield the title compound as a solid.
Sources & evidence
- ORD record
- ord-c071461b9918485586eb55d21fbc4f31
- Source dataset
- uspto-grants-2015_04
- Patent number
- US09018175B2
Reaction notes
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