Methanesulfonic Acid → HCID 118351606, compound

HRID 1477085Notes

Reaction equation

HRID 1477085 reaction equation
[C:1](=[O:14])([O:3][CH2:4][CH:5]([NH2:13])[CH2:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)[NH2:2].[O-:15][C:16]#[N:17].[Na+].CS(O)(=O)=O>ClCCl>[NH2:17][C:16]([NH:2][C:1](=[O:14])[O:3][CH2:4][CH:5]([NH2:13])[CH2:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)=[O:15]

Participants

5

Reactant 3

HCID 6395Methanesulfonic AcidHCID 517096Sodium CyanateHCID 11708214178429-61-3

Product 1

HCID 118351606HCID 118351606, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

As shown in Scheme II, 2-amino-3-phenylpropyl carbamate (V) is reacted with sodium cyanate and methansulfonic acid in dichloromethane, to give 2-amino-3-phenylpropyl (aminocarbonyl)carbamate (VI).

Sources & evidence

ORD record
ord-c3bcf03026174c18ac8352085e2dbcb7
Source dataset
uspto-grants-2016_08
Patent number
US09403761B2

Reaction notes

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