HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 178462646, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 1-Ethylpiperazine | HCID 79196 | — |
| Reactant | HCID 178424653 | HCID 178424653 | — |
| Product | HCID 178462646 | HCID 178462646 | — |
Reaction Steps
The title compound is prepared from 4-cyano-1H-imidazole-2-carboxylic acid [2-(4,4-dimethyl-cyclohex-1-enyl)-6-(1-hydroxy-cyclopentyl)-pyridin-3-yl]-amide (as prepared in the previous step), N-ethylpiperazine, and thionyl chloride in DCM solvent according to the procedure in Example 43.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09403804B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-5c9590aad18d4e22814c6a46aa03ad52 |
| Source note | uspto-grants-2016_08 |