HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 136954683, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 11045887 | HCID 11045887 | — |
| Product | HCID 136954683 | HCID 136954683 | 101.1% |
Reaction Steps
tert-Butyl 4-(4,6-dichloro-1,3,5-triazin-2-yl)piperazine-1-carboxylate (14.9 g, 44.5 mmol) synthesized in Reference Synthesis Example 5 and 1 M sodium hydroxide aqueous solution (111 mL, 111 mmol) were used to obtain the title compound (14.2 g, quantitative) by synthesis in a similar manner to Reference Synthesis Example 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09403798B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-b252e6ea1154415c822d757d05cd6361 |
| Source note | uspto-grants-2016_08 |