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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1477569Generated: October 29, 2026

HCID 136954683, compound → HCID 178452267, compound

https://huagongshe.com/reaction/1477569

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 136954683HCID 136954683—
CatalystPalladium hydroxideHCID 9942167—
ProductHCID 178452267HCID 178452267—

Reaction Steps

tert-Butyl 4-(6-chloro-4-oxo-4,5-dihydro-1,3,5-triazin-2-yl)piperazine-1-carboxylate (14.2 g, 45.0 mmol) synthesized in Reference Synthesis Example 6 and palladium hydroxide-activated carbon catalyst (142 mg) were used to obtain a crude product of the title compound by synthesis in a similar manner to Reference Synthesis Example 3. The crude product was used in the next reaction as it was.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09403798B2
Source datasetuspto-grants-2016_08
ORD IDord-988b6248acd648f6975c5479586ebd03
Source noteuspto-grants-2016_08