HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 136954683, compound → HCID 178452267, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 136954683 | HCID 136954683 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Product | HCID 178452267 | HCID 178452267 | — |
Reaction Steps
tert-Butyl 4-(6-chloro-4-oxo-4,5-dihydro-1,3,5-triazin-2-yl)piperazine-1-carboxylate (14.2 g, 45.0 mmol) synthesized in Reference Synthesis Example 6 and palladium hydroxide-activated carbon catalyst (142 mg) were used to obtain a crude product of the title compound by synthesis in a similar manner to Reference Synthesis Example 3. The crude product was used in the next reaction as it was.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09403798B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-988b6248acd648f6975c5479586ebd03 |
| Source note | uspto-grants-2016_08 |