HCID 117839986, compound → HCID 117839488, compound

Participants

Reaction Steps

To an ethanol solution (2.6 mL) of 1-(4-fluorophenyl)-3-nitro-1H-pyrrole (131 mg, 0.635 mmol) synthesized in Reference Synthesis Example 248, palladium-activated carbon (13.1 mg) was added and the resultant mixture was stirred under hydrogen atmosphere at room temperature for 1 day. After completion of the reaction, the reaction solution was filtered with Celite and the filtrate was concentrated under reduced pressure to obtain the title compound as a crude product.

Provenance & Evidence