Sodium Bicarbonate → HCID 67870438, compound

Participants

Reaction Steps

To a crude product synthesized by using tert-butyl 4-(4-methylthiophen-2-yl)-5,6-dihydropyridine-1(2H)-carboxylate (10.0 mg, 0.358 mmol) in a similar manner to Reference Synthesis Example 26, saturated sodium bicarbonate aqueous solution was added and extraction from the resultant mixture with ethyl acetate was performed. The organic layer was washed with water, dried over anhydrous sodium sulfate, and concentrated under reduced pressure to obtain a crude product of the title compound.

Provenance & Evidence