HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl orthoformate → HCID 117839443, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl orthoformate | HCID 31214 | — |
| Reactant | HCID 140668404 | HCID 140668404 | — |
| Product | HCID 117839443 | HCID 117839443 | 76% |
Reaction Steps
Methyl N-({[(5-bromothiophen-2-yl)methyl]amino}carbonyl)-carbamimidothioate (700 mg, 2.27 mmol) synthesized in Reference Synthesis Example 295 and triethyl orthoformate were used to obtain the title compound (547 mg, yield 76%) by synthesis in a similar manner to Reference Synthesis Example 292.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09403798B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-104fb0f4ef884b2d95f6adc374babdf1 |
| Source note | uspto-grants-2016_08 |