HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl piperazine-1-carboxylate → HCID 117849156, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl piperazine-1-carboxylate | HCID 143452 | — |
| Reactant | HCID 117839530 | HCID 117839530 | — |
| Product | HCID 117849156 | HCID 117849156 | 97.1% |
Reaction Steps
6-Methyl-4-(methylthio)-1-{[5-(trifluoromethyl)thiophen-2-yl]methyl}-1,3,5-triazin-2(1H)-one (309 mg, 0.962 mmol) synthesized in Reference Synthesis Example 292 and tert-butyl piperazine-1-carboxylate (269 mg, 1.44 mmol) were used to obtain the title compound (429 mg, yield 97%) by synthesis in a similar manner to Reference Synthesis Example 348.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09403798B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-2fcf709f23424c38b53998b0650bc372 |
| Source note | uspto-grants-2016_08 |