HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-5-(trifluoromethyl)pyridine → HCID 117839830, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-5-(trifluoromethyl)pyridine | HCID 92342 | — |
| Reactant | HCID 117839396 | HCID 117839396 | — |
| Product | HCID 117839830 | HCID 117839830 | 3.8% |
Reaction Steps
1-(4-chlorobenzyl)-4-(piperazin-1-yl)-1,3,5-triazin-2(1H)-one (31 mg, 0.10 mmol) synthesized in Reference Synthesis Example 9 and 2-chloro-5-trifluoromethylpyridine (18 mg, 0.10 mmol) in a similar manner to Synthesis Example 76 to obtain the title compound (1.7 mg, yield: 3.7%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09403798B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-97882bea76fa4f84a0b2bfec8ab44a32 |
| Source note | uspto-grants-2016_08 |