HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1477763Generated: November 3, 2026
Benzoyl isothiocyanate → HCID 86688406, compound
https://huagongshe.com/reaction/1477763
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzoyl isothiocyanate | HCID 68284 | — |
| Reactant | 2-methyl-4,5,6,7-tetrahydro-2H-indazol-3-amine | HCID 52903608 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 86688406 | HCID 86688406 | — |
Reaction Steps
To a solution of compound 124 (5.44 g, 33.1 mmol) in 40 mL of acetone at 0° C. was added dropwise benzoyl isothiocynate (5.4 g, 33.1 mmol). The reaction mixture was gradually warmed up and stirred in an oil bath of 60° C. until TLC indicated there was no starting material remained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09403815B2 |
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| Source dataset | uspto-grants-2016_08 |
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| ORD ID | ord-0ed7ae02d4164ea190e614c3bb22e5df |
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| Source note | uspto-grants-2016_08 |
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