huagongshe.com
HRID1477777

反应详情

EQUATION

反应方程式

HRID 1477777 的结构方程式

REACTANTS

反应物

2
结构：CCC(C)(N)CO
HCID10154017

2-amino-2-methylbutan-1-ol

C5H13NO

结构：O=C(O)c1cnc(C2CC2)c(OCC2CC2)n1
HCID86682331

未命名化合物

PRODUCTS

生成物

1
结构：CCC(C)(CO)NC(=O)c1cnc(C2CC2)c(OCC2CC2)n1
HCID71525575

未命名化合物

PROCEDURE

实验过程

The title compound was synthesized in analogy to Example 8e, using 5-cyclopropyl-6-cyclopropylmethoxy-pyrazine-2-carboxylic acid (Example 10 g, 100 mg, 0.43 mmol) and 2-amino-2-methyl-1-butanol (CAN 10196-30-2, 64.74 mg, 0.64 mmol) as starting materials, and isolated (12 mg, 8.79%) as off white solid, LC-MS (UV peak area, ESI) 100%, 320.4 (M+H).

WORKUP

后处理

  1. customisolated (12 mg, 8.79%) as off white solid, LC-MS (UV peak area, ESI) 100%, 320.4 (M+H)