HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-2-ethyl-N-methyl-butyramide → HCID 71526038, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-2-ethyl-N-methyl-butyramide | HCID 79810370 | — |
| Reactant | 5-Cyclopropyl-6-cyclopropylmethoxy-pyrazine-2-carboxylic acid | HCID 86682331 | — |
| Product | HCID 71526038 | HCID 71526038 | — |
Reaction Steps
The title compound was synthesized in analogy to Example 15, using 5-cyclopropyl-6-cyclopropylmethoxy-pyrazine-2-carboxylic acid (Example 10 g; 100 mg, 0.42 mmol) and 2-amino-2-ethyl-N-methyl-butyramide (78.2 mg, 0.64 mmol) as starting materials, and isolated (12 mg, 9.44%) as colorless sticky solid, LC-MS (UV peak area, ESI) 97.47%, 361.4 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09403808B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-9378d49c7dcd4fae988edd87011e7c1c |
| Source note | uspto-grants-2016_08 |