HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 83906267, compound → HCID 71526315, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 83906267 | HCID 83906267 | — |
| Reactant | 5-Cyclopropyl-6-cyclopropylmethoxy-pyrazine-2-carboxylic acid | HCID 86682331 | — |
| Product | HCID 71526315 | HCID 71526315 | — |
Reaction Steps
The title compound was synthesized in analogy to Example 69, using 5-cyclopropyl-6-cyclopropylmethoxy-pyrazine-2-carboxylic acid (Example 10 g 10 mg, 0.043 mmol) and 1,1-dimethyl-3-pyridin-4-yl-butylamine (12 mg, 0.064 mmol) as starting materials and isolated (10 mg, 59.38%) as white solid; LC-MS (UV peak area, ESI) 99.2%, 395.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09403808B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-9723ed3509f84fd994da00a5996583e2 |
| Source note | uspto-grants-2016_08 |