HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 43559029, compound → HCID 71526404, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 43559029 | HCID 43559029 | — |
| Reactant | 5-Cyclopropyl-6-cyclopropylmethoxy-pyrazine-2-carboxylic acid | HCID 86682331 | — |
| Product | HCID 71526404 | HCID 71526404 | — |
Reaction Steps
The title compound was synthesized in analogy to Example 69, using 5-cyclopropyl-6-cyclopropylmethoxy-pyrazine-2-carboxylic acid (Example 10 g, 100 mg, 0.42 mmol) and 1-methyl-1-(5-methyl-thiazol-2-yl)-ethylamine (100 mg, 0.64 mmol) as starting materials and isolated (29 mg, 18.3%) as white solid; LC-MS (UV peak area, ESI) 94.85%, 372.8 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09403808B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-05bb6a8ddd1f41a28577298222f97cee |
| Source note | uspto-grants-2016_08 |