HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-methoxy-2-methylbutan-2-amine → HCID 71526495, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-methoxy-2-methylbutan-2-amine | HCID 22344990 | — |
| Reactant | 5-Cyclopropyl-6-cyclopropylmethoxy-pyrazine-2-carboxylic acid | HCID 86682331 | — |
| Product | HCID 71526495 | HCID 71526495 | — |
Reaction Steps
The title compound was synthesized in analogy to Example 69 using 5-cyclopropyl-6-cyclopropylmethoxy-pyrazine-2-carboxylic acid (Example 10 g, 50 mg, 0.214 mmol) and 3-methoxy-1,1-dimethyl-propylamine (CAN 889765-21-3, 50 mg, 0.32 mmol) as starting materials and isolated (40 mg, 56.14%) as white solid; LC-MS (UV peak area, ESI) 99.87%, 333.8 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09403808B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-627167c854cd4822bfbb0b656338fd9c |
| Source note | uspto-grants-2016_08 |